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Structural properties of size-controlled SnO2 nanopowders produced by sol-gel method

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dc.contributor.authors Kose, H; Karaal, S; Aydin, AO; Akbulut, H;
dc.date.accessioned 2020-10-16T11:10:34Z
dc.date.available 2020-10-16T11:10:34Z
dc.date.issued 2015
dc.identifier.citation Kose, H; Karaal, S; Aydin, AO; Akbulut, H; (2015). Structural properties of size-controlled SnO2 nanopowders produced by sol-gel method. MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING, 38, 412-404
dc.identifier.issn 1369-8001
dc.identifier.uri https://doi.org/10.1016/j.mssp.2015.03.028
dc.identifier.uri https://hdl.handle.net/20.500.12619/69920
dc.description.abstract SnO2 nanoparticles were synthesized by sol-gel method with different sol concentrations and the effect of sol concentration on the structural properties of SnO2 was investigated. The aim of this work is synthesizing of SnO2 nanoparticles from SnCl2 center dot 2H(2)O (tin (II) chloride dihydrate) precursor to obtain high quality powders for using as Li-ion anode material. For this purpose, during the SnO2 precursor solution preparation, chloride ions were removed from the solution and then the sol-gel synthesis was applied. Produced SnO2 nanopowders were characterized by x-ray diffraction (XRD), field emission gun scanning electron microscopy (FEG-SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and energy dispersive x-ray spectroscopy (EDS) analyses. TG-DTA and FT-IR analysis were performed on the synthesized sol. Grain size, crystal index and lattice strains of SnO2 particles were calculated. The results showed that the grain size of particles has increased by the increasing of sol concentration, and the crystallinity has been improved. The smallest crystallite size (6.03 nm) was obtained from the SnO2 sample of 6 mmole concentration sol and maximum size (9.65 nm) from 14 mmole sol according to W-H analysis. (C) 2015 Elsevier Ltd. All rights reserved.
dc.language English
dc.publisher ELSEVIER SCI LTD
dc.subject Physics
dc.title Structural properties of size-controlled SnO2 nanopowders produced by sol-gel method
dc.type Proceedings Paper
dc.identifier.volume 38
dc.identifier.startpage 404
dc.identifier.endpage 412
dc.contributor.saüauthor Köse, Hilal
dc.contributor.saüauthor Dombaycıoğlu, Şeyma
dc.contributor.saüauthor Aydın, Ali Osman
dc.contributor.saüauthor Akbulut, Hatem
dc.relation.journal MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING
dc.identifier.wos WOS:000357839800060
dc.identifier.doi 10.1016/j.mssp.2015.03.028
dc.identifier.eissn 1873-4081
dc.contributor.author Köse, Hilal
dc.contributor.author Dombaycıoğlu, Şeyma
dc.contributor.author Aydın, Ali Osman
dc.contributor.author Akbulut, Hatem


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